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Field Sampling Plan

Table 2.2 - Sample Container, Methods, Preservation, and Holding Times for Aqueous Samples

Parameters

Analytical Method

Sample Container

Preservation

Holding Times

Volatile Organic Compounds

SW8260A

Three 40-mL glass vials with Teflon-lined septum

HCl to pH<2; Cool to 4�C�2�C

14 days

Semivolatile Organic Compounds

SW8270B

One 1-liter widemouth amber glass jar with Teflon-lined lid

Cool to 4�C�2�C

Extract within 7 days of collection and analyze within 40 days of extraction

Explosives

SW8330 (lab modified)

One 1-liter widemouth amber glass jar with Teflon-lined lid

Cool to 4�C�2�C; Store in the dark

Extract within 7 days of collection and analyze within 40 days of extraction

ICP Metals (Barium, Chromium, Copper, Nickel, Zinc)

SW6010A

One 500 mL plastic bottle

HNO3 to pH<2; Cool to 4�C�2�C

180 days

Arsenic, Cadmium, Lead

SW7060A, SW7131, SW7421

One 500 mL plastic bottle

HNO3 to pH<2; Cool to 4�C�2�C

180 days

Mercury

SW7470A

One 500 mL plastic bottle

HNO3 to pH<2; Cool to 4�C�2�C

13 days

HNO3 = nitric acid